研究论文
Assembly of the Nosiheptide A-Ring: A Fruitful Lesson
Hans‐Dieter Arndt, Jin‐Yong Lu, Matthias Riedrich, K. Philip Wojtas
Friedrich Schiller University Jena TU Dortmund University
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摘要 · 完整
The synthesis of a 28-membered thiopeptide macrocycle is described. Key steps are mild aza-Wittig thiazole ring closures, a scandium(III)-mediated regioselective ester hydrolysis, and a highly efficient macrolactam formation with its 3-hydroxypyridine nucleus orthogonally protected.
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化学Carbohydrate Chemistry and Synthesis
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